The CRR houses state-of-the-art equipment for PhD and post-doctoral researchers to conduct radiochemistry research spanning environmental speciation, analytical science, coordination chemistry, nuclear forensics and decommissioning.
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Over the barrier
- Absorption spectroscopy: UV-Vis-niR – Shimadzu UV1800 UV-spectrophotometer (200 – 1800 nm). (https://en.wikipedia.org/wiki/Absorption_spectroscopy)
- Infra-red spectrometer, Fourier Transform Infrared spectroscopy (FT-IR), Perkin Elmer Spectrum RX1 spectrometer with an ATR attachment. (https://en.wikipedia.org/wiki/Fourier_transform_infrared_spectroscopy)
- NMR spectroscopy: Bruker Avance 400 MHz spectrometer with a multinuclear BBO probe variable temperature unit and automation.Field Flow Fractionation, Particle separation analyser: Postnova AF2000 Focus Field Flow Fractionater (https://en.wikipedia.org/wiki/Field_flow_fractionation)
Quantification of Radionuclides:
Liquid scintillation counting (https://en.wikipedia.org/wiki/Liquid_scintillation_counting)
- Liquid scintillation spectrometer (alpha and beta): Quantulus Ultra Low Level Liquid Scintillation Counter
- Liquid scintillation spectrometer (alpha, beta and gamma): Packard Tri-Carb 1900 TR Liquid Scintillation Counter
Gamma Spectroscopy (https://en.wikipedia.org/wiki/Gamma_spectroscopy)
- High performance Gamma Ray Detector: ORTEC HPGe Gamma Ray Detector (Möbius Recycler)
- Canberra Low Energy HPGe Gamma Ray Detector
- Canberra Coaxial HPGe Gamma Ray Detector
Alpha and Beta Spectroscopy (http://www.canberra.com/products/detectors/pips-detectors.asp)
- 6 x Alpha Passivated Implanted Planar Silicon (PIPS®) detectors: Canberra, model A450
- Various perspex glove boxes (N2, Ar, or CO2 free O2 atmospheres) for environmental radiochemistry research.
- Negative atmosphere glove box facilities for aqueous and non-aqueous 237Np work.
- Autoradiography: Typhoon 9410 variable mode imager with BAS-IP MS storage phosphor screens (https://en.wikipedia.org/wiki/Autoradiograph)
- Raman spectroscopy: Horiba XploRA PLUS V1.2 Å MULTILINE Confocal Raman microscope with 532 nm, 638 nm and 785 nm solid state lasers. (https://en.wikipedia.org/wiki/Raman_spectroscopy)
- Luminescence spectroscopy: Edinburgh Instrument FP920 Phosphorescence Lifetime Spectrometer with a tunable 450 watt steady state xenon lamp, a 5 watt microsecond pulsed xenon flashlamp, plug and play 375 nm, 405 nm, 640 nm and 980 nm picosecond pulsed diode lasers, a Fianium tunable supercontinuum laser, a red sensitive visible photomultiplier detector, a liquid nitrogen cooled near infra-red detector (800 – 1700 nm), integrating sphere and sample housing for room temperature solution measurements, liquid nitrogen temperature frozen solution measurements and solid state sample measurements. Lifetime measurements range from sub nanoseconds to milliseconds. (https://en.wikipedia.org/wiki/Fluorescence_spectroscopy)
- Upright fluorescence microscope, Leica microsystems DM2700 M. (https://en.wikipedia.org/wiki/Fluorescence_microscope)
General Uranium and Thorium Chemistry Labs
General synthetic chemistry capabilities (inorganic and organic), plus:
- Multiple Schlenk line apparatus for air sensitive manipulations (ground glass and Teflon taps)
- Solvent distillation apparatusSublimation apparatus3 x inert atmosphere positive pressure glove boxes, Innovative Technologies, argon or nitrogen (2 gloves each) with integrated -35 degrees Celcius freezer.
- Photolysis equipment: including broad band medium pressure Hg lamp and visible filter with 400W and 600W settings for small scale photolysis experiments.
- Cyclic voltammetry equipment (Metrohm microAutolab3). (https://en.wikipedia.org/wiki/Cyclic_voltammetry)
Access to other Chemistry facilities:
- University high performance computing clusters
- Single crystal X-Ray Diffraction (U, Th, Np)
- Elemental analysis (U and Th only)
- Solvent drying column purification system (Innovative Technologies)
- National EPR service (U and Th only)
- Magnetic measurements: Superconducting Quantum Interference Device, SQUID (U and Th only)
- Ultra-fast laser lab, UF-2 (U, Th and Np)